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/Title ({Determination of low alloying element concentrations in cast iron by laser induced breakdown spectroscopy based on TEA CO2 laser system})
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2017-10
{Determination of low alloying element concentrations in cast iron by laser induced breakdown spectroscopy based on TEA CO2 laser system}
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bibtex/bibtexkey/Savovic2017
Jelena Savovic
Sanja Zivkovic
Milos Momcilovic
Milan Trtica
Milovan Stoiljkovic
Miroslav Kuzmanovic
The analytical capability of laser-produced plasma for the analysis of low alloying elements in cast iron samples has been investigated. The plasma was induced by irradiation of a sample in air at atmospheric pressure using an infrared CO 2 laser. Emission spectra were recorded by time-integrated spatially-resolved measurement technique. A set of ten cast iron samples in a powder or particulate form were provided by BAM (Bundesanstalt f{\"{u}}r Material forschung und pr{\"{u}}fung, Deutschland), seven of which were used for calibration, and three were treated as unknowns. Linear calibration curves were obtained for copper, chromium, and nickel, with correlation coefficients above 0.99. Precision and accuracy of the LIBS method was evaluated and compared to those obtained by the inductively coupled plasma (ICP) analysis of the same samples. Detection limits for Cu, Cr and Ni were close to those reported in the literature for other comparable iron-based alloys obtained using different LIBS systems. Analytical figures of merit of the studied LIBS system may be considered as satisfying, especially in the light of other advantages of the method, like cost effective and fast analysis with no sample preparation, and with a possibility for real-time on-site analysis.
10.2298/JSC170303073S
application/pdf
Article
Jelena Savovic
Sanja Zivkovic
Milos Momcilovic
Milan Trtica
Milovan Stoiljkovic
Miroslav Kuzmanovic
Savovic2017
10.2298/JSC170303073S
:C$backslash$:/Users/Dekanski/AppData/Local/Mendeley Ltd./Mendeley Desktop/Downloaded/Savovic et al. - 2017 - Determination of low alloying element concentrations in cast iron by laser induced breakdown spectroscopy based.pdf;:05_4775_4029.pdf:PDF
Journal of the Serbian Chemical Society
oct
10
1135--1145
{Determination of low alloying element concentrations in cast iron by laser induced breakdown spectroscopy based on TEA CO2 laser system}
http://www.doiserbia.nb.rs/Article.aspx?ID=0352-51391700073S
82
2017
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