Undecanol–ethanol–water ternary system-based microextraction for the detection of cadmium (Short communication)

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Published: Apr 28, 2019
DOI: https://doi.org/10.2298/JSC180831110U
Keywords:
eco-friendly GFAAS microextraction heavy metal ions

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Oya Aydın Urucu
Marmara University, Faculty of Science and Letters, Chemistry Department, Goztepe Campus, 34722, Istanbul
Ece Kök Yetimoğlu
Marmara University, Faculty of Science and Letters, Chemistry Department, Goztepe Campus, 34722, Istanbul
Şeyda Dönmez
Marmara University, Faculty of Science and Letters, Chemistry Department, Goztepe Campus, 34722, Istanbul
Sabahattin Deniz
Marmara University, Faculty of Technology, Textile Engineering Department, Goztepe Campus, 34722, Istanbul

Abstract

An eco-friendly, simple, and sensitive solidification of floating organic drop based dispersive liquid–liquid microextraction (SFODME) procedure was intro­duced for the separation and preconcentration of cadmium. After 2-(5-bromo-
-2-pyri­dylazo)-5-(diethylamino)phenol (5-Br-PADAP) was complexed with cad­mium ions in sample, the undecanol–ethanol–water ternary system was used as an organic solvent for extraction. The main factors relevant to the microextraction efficiency such as pH, concentration of 5-Br-PADAP, amount of extraction solvent were optimized. The detection limit is 0.01 µg L-1 along with preconcentration factor 266. The recovery of the analyte was between 98 % and 103 %, with relative standard deviation below 6 %. The developed procedure was successfully tested on the analysis of water, hair dye, and food samples.

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How to Cite
[1]
O. Aydın Urucu, E. Kök Yetimoğlu, Şeyda Dönmez, and S. Deniz, “Undecanol–ethanol–water ternary system-based microextraction for the detection of cadmium (Short communication)”, J. Serb. Chem. Soc., vol. 84, no. 4, pp. 435–443, Apr. 2019.
Issue
Vol. 84 No. 4 (2019)
Section
Environmental Chemistry

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