Preparation of composite zein/natural resin nanoparticles

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Published: Mar 30, 2020
DOI: https://doi.org/10.2298/JSC190401071S
Keywords:
zein shellac rosin biopolymer encapsulation

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Ljiljana Spasojević
University of Novi Sad, Faculty of Technology Novi Sad, Bulevar cara Lazara 1, 21000 Novi Sad
Jaroslav Katona
University of Novi Sad, Faculty of Technology Novi Sad, Bulevar cara Lazara 1, 21000 Novi Sad
Sandra Bučko
University of Novi Sad, Faculty of Technology Novi Sad, Bulevar cara Lazara 1, 21000 Novi Sad
Lidija Petrović
University of Novi Sad, Faculty of Technology Novi Sad, Bulevar cara Lazara 1, 21000 Novi Sad
Jelena Milinković Budinčić
University of Novi Sad, Faculty of Technology Novi Sad, Bulevar cara Lazara 1, 21000 Novi Sad
Jadranka Fraj
University of Novi Sad, Faculty of Technology Novi Sad, Bulevar cara Lazara 1, 21000 Novi Sad
Altynay Sharipova
Kazakh National Research Technical University, Almaty
Saule Aidarova
Kazakh National Research Technical University, Almaty, Kazakh–British Technical University, Almaty

Abstract

The aim of this work was to investigate a possibility of preparing composite zein/natural resin (shellac and rosin) nanoparticles by antisolvent co–precipitation from their aqueous ethanol solutions. Influence of zein/resin mass ratio (1/0, 0.8/0.2, 0.5/0.5, 0.4/0.6 and 0/1) and pH (2–12) on particle size, d, and zeta potential, z, of the prepared particles was studied. The func­tional properties of zein/rosin composite nanoparticles were evaluated by studying carvacrol encapsulation. It was shown that the antisolvent precipit­ation can be successfully used to prepare the shellac and rosin nanoparticles, as well as the composite zein/shellac and the zein/rosin nanoparticles. Colloidal properties, d and z, of the obtained nanoparticles are influenced by the zein/
/resin mass ratio and the pH of nanoparticles dispersions. The isoelectric point of composite nanoparticles can be modulated by varying the zein/resin mass ratio. It was found that the zein/rosin nanoparticles are suitable for carvacrol encapsulation, where carvacrol release is enhanced by increasing the rosin share in the composite zein/rosin nanoparticles.

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How to Cite
[1]
L. Spasojević, “Preparation of composite zein/natural resin nanoparticles”, J. Serb. Chem. Soc., vol. 85, no. 3, pp. 369–380, Mar. 2020.
Issue
Vol. 85 No. 3 (2020)
Section
Materials

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